Analytical Instrument Documents

No-D NMR (No-Deuterium Proton NMR) technique is a measurement of high resolution 1H NMR spectra without deuterium solvent. It suggests that any reaction mixture or reagent solution are directly available for No-D NMR measurement.

In this article, we will show the accurate measurements of the diffusion coefficients (D) by using room-temperature ionic liquids (RTIL, IL) as examples.

13C NMR spectra provide wide range chemical shift, and it suggests that can easily distinguish each signals. But carbon resolution of 2D spectra such as HSQC and HMBC is worse than 1D 13C spectra due to small data points. In order to analyze a compound with close 13C chemical shifts, a high resolution 2D spectrum is required frequently. In this document, some improvements to distinguish each signals on 13C axis of 2D hetero nuclear experiments are presented.

POMMIE (Phase Osacillations to Maximize Editing) is a 13C experiment that, like the more familiar DEPT experiment, utilizes polarization transfer to enhance the intensities of the 13C signals. However, unlike DEPT, POMMIE edits the spectrum by varying pulse phase rather than adjusting pulse flip angle.

"pure shift" is  method for homo nuclear broad band decoupling. Sensitivity would be reduced, but spectra of only (pure) chemical shifts can be obtained by eliminating j coupling.

"pure shift" is  method for homo nuclear broad band decoupling. Sensitivity would be reduced, but spectra of only (pure) chemical shifts can be obtained by eliminating j coupling.

"pure shift" is  method for homo nuclear broad band decoupling. Sensitivity would be reduced, but spectra of only (pure) chemical shifts can be obtained by eliminating j coupling.

The applications for lithium ion batteries (LIB) cover a wide range, from power sources for personal computers and mobile devices to automobiles, and there is always a demand for even better performance and safety. In order to ensure the performance and quality of LIB, analysis and evaluation using high-performance assessment systems is necessary. JEOL offers a full line-up of equipment to support the development of new LIB technologies and to improve product quality, including instruments for morphology observation and surface analysis, chemical analysis systems to perform structural analysis on a molecular level, as well as fabrication systems to create high-performance coatings and powders. This LIB note offers solutions for researchers and engineers who are looking for the best equipment for their application.

JEOL offers numerous analytical tools to support both "food safety & security" as well as various evaluations of primary, secondary and tertiary functions of foodstuffs which are useful for a wide range of users associated with this field. This Foodnote introduces the features of each of the instruments and actual analysis examples, and is designed for researchers and engineers who are considering purchases of instruments. This brochure also presents comprehensive evaluations and analysis solutions that can be achieved with combinations of multiple instruments.

This Bionote presents an overview of the basics, namely principles and features of various instruments, as well as application examples using numerous optional attachments. We hope that the Bionote will assist researchers and engineers who intend to perform analyses in finding and exploring new approaches.