Analytical Instrument Documents

Applications concerning Polymers, Materials & Chemistry using the SpiralTOF.

Applications for Life Science using the SpiralTOF.

Applications concerning MALDI MS Imaging using the SpiralTOF.

Various applications on the topics of Materials and Chemistry for the AccuTOF GC Series

Publication containing various applications pertaining to Environment, Food, Flavor, & Fragrance.

Notebook containing various articles and application notes pertaining to the AccuTOF DART.

The ROSY (Relaxation Ordered SpectroscopY) is a method in which the 13C CPMAS spectrum of a mixture is classified by a longitudinal relaxation time of 1H, and the 13C CPMAS spectrum is displayed separately for each substance. In solution NMR, each peak in the 1H spectrum has its own longitudinal relaxation time. In solid-state NMR, however, spin diffusion occurs due to the dipolor interaction between 1H, and all 1H have the same longitudinal relaxation in the domain within a certain distance. The 13C spectrum can be separated for each domain by using this difference in relaxation time of 1H. The longitudinal relaxation time (T1H) obtained by the saturation recovery method as shown in Fig.1a is usually used to separate the 13C spectrum of the mixture. The size of the domain that can be separated by this method is about 100 nm. To separate domains smaller than this, a measurement using the relaxation time at rotational flame (T1ρH) obtained by the spinlock method as shown in Fig.1b is effective. The domain size that can be separated by T1ρH is about several nm, and it is possible to determine the phase separation structure of block copolymers and the molecular compatibility.

This study presents a comprehensive method for the analysis of gas chromatograph (GC)-amendable pesticides in Cannabis flower. Furthermore, this method uses dispersive solid phase extraction (dSPE) to help mitigate matrix effects that are common in the flower extract. Three selected reaction monitoring (SRM) transitions were used for each target pesticide. This study was focused on developing a robust and sensitive method for GC amendable pesticides in Cannabis flower for use in the state of California. However, LC-MS/MS would also be required to analyze the complete California pesticide list.

Pursuing the ultimate in performance and functionality. The JMS-T2000GC AccuTOF™ GC-Alpha Time-of-Flight Mass Spectrometer takes you to a new world of mass spectrometry, the ultimate GC-MS with superior performance and ease of operation.

Interaction between microwave photon and spins means in other words, interaction between resonating photon in a closing space and spins. Thus, measuring spectra using a non-resonant device can prevent the Purcell effect or strong coupling from distortion of intrinsic spectra. Figure 1(a) is a drawing expressing a typical spectroscopy. A light source irradiates light to a sample, and transmitted light is detected. A simple and non-resonant wave guide, as shown in Fig.1(b), can provide absorption spectra of para- and ferromagnetic samples which have a high spin density.